The static aging effect on the seedless synthesis of different ranges FAU-type zeolite Y at various factors
DOI:
https://doi.org/10.31699/IJCPE.2019.4.2Keywords:
Faujasite-type, static aging, seedless synthesis, zeolite, hydrothermal treatmentAbstract
This work investigates generating of pure phase Faujasite-type zeolite Y at the ranges chosen for this study via a static aging step in the absence of seeds synthesis. Nano-sized crystals may result when LUDOX AS-40 is used as a silica source for gel composition of range 6 and the crystallization step may be conducted for a period of 4 to 19 hr at 100 ⁰C. Moreover, large-crystals with high crystallinity pure phase Y zeolite can be obtained at hereinabove conditions but when hydrous sodium metasilicate is used as a silica source. The other selected ranges also offer pure phase Y zeolite at the same controlled conditions.
References
Aimen Isa, M., Chew, T.L., Yeong, Y.F.: Zeolite NaY synthesis by using sodium silicate and colloidal silica as silica source. IOP Conf. Ser. Mater. Sci. Eng. 458, (2018).
Al-Jubouri, S.M., de Haro-Del Rio, D.A., Alfutimie, A., Curry, N.A., Holmes, S.M.: Understanding the seeding mechanism of hierarchically porous zeolite/carbon composites. Microporous Mesoporous Mater. 268, 109–116 (2018).
Wittayakun, J., Khemthong, P., Prayoonpokarach, S.: Synthesis and characterization of zeolite NaY from rice husk silica. Korean J. Chem. Eng. 25, 861–864 (2008).
Edanol, Y., Usman, K., Buenviaje, S., Mantua, M., Payawan, L.: Utilizing silica from rice hull for the hydrothermal synthesis of zeolite Y. KIMIKA. 29, 17–21 (2018).
Al-Jubouri, S.M., Waisi, B.I., Holmes, S.M.: Rietveld texture refinement analysis of linde type a zeolite from X-ray diffraction data. J. Eng. Sci. Technol. (2018)
Dyer, A.: Zeolites, (2001)
Kovo, A.S., Hernandez, O., Holmes, S.M.: Synthesis and characterization of zeolite Y and ZSM-5 from Nigerian Ahoko kaolin using a novel, lower temperature, metakaolinization technique. J. Mater. Chem. 19, 6207–6212 (2009)
Azizi, S.N., Daghigh, A.A., Abrishamkar, M.: Phase transformation of zeolite P to Y and analcime zeolites due to changing the time and temperature. J. Spectrosc. 2013, 1–5 (2013).
Rahman, M.M., Hasnida, N., Wan Nik, W.B.: Preparation of zeolite Y using local raw material rice husk as a silica source. J. Sci. Res. 1, 285–291 (2009).
Holmberg, B. a., Wang, H., Norbeck, J.M., Yan, Y.: Controlling size and yield of zeolite Y nanocrystals using tetramethylammonium bromide. Microporous Mesoporous Mater. 59, 13–28 (2003).
Li, Q., Zhang, Y., Cao, Z., Gao, W., Cui, L.: Influence of synthesis parameters on the crystallinity and Si/Al ratio of NaY zeolite synthesized from kaolin. Pet. Sci. 7, 403–409 (2010).
Ahmedzeki, N.S., Al-tabbakh, B.A.: Catalytic reforming of Iraqi naphtha over Pt-Ti / HY zeolite catalyst. Iraqi J. Chem. Pet. Eng. 17, 45–56 (2016)
García-Martínez, J., Li, K., Krishnaiah, G.: A mesostructured Y zeolite as a superior FCC catalyst – from lab to refinery. Chem. Commun. 48, 11841 (2012).
Zhao, J., Yin, Y., Li, Y., Chen, W., Liu, B.: Synthesis and characterization of mesoporous zeolite Y by using block copolymers as templates. Chem. Eng. J. 284, 405–411 (2016).
Bortolatto, L.B., Boca Santa, R.A.A., Moreira, J.C., Machado, D.B., Martins, M.A.P.M., Fiori, M.A., Kuhnen, N.C., Riella, H.G.: Synthesis and characterization of Y zeolites from alternative silicon and aluminium sources. Microporous Mesoporous Mater. 248, 214–221 (2017).
Gazola, F.C., Pereira, M.R., Barros, M. a S.D., Silva, E. a., Arroyo, P. a.: Removal of Cr3+ in fixed bed using zeolite NaY. Chem. Eng. J. 117, 253–261 (2006).
Ostroski, I.C., Barros, M.A.S.D., Silva, E.A., Dantas, J.H., Arroyo, P.A., Lima, O.: A comparative study for the ion exchange of Fe (III) and Zn (II) on zeolite NaY. J. Hazard. Mater. 161, 1404–1412 (2009)
Al-jubouri, S.M., Adil, H., Lafta, H.A., Waisi, B.I.: Effect of synthesis parameters on the formation 4A zeolite crystals : characterization analysis and heavy metals uptake performance study for water treatment. 165, 290–300 (2019).
Cejka, J., VAN Bekkum, H., Corma, A., Schüth, F. eds: Introduction to zeolite science and practice. Elsevier, UK (2007)
Kovo, A.S., Holmes, S.M.: Effect of aging on the synthesis of kaolin-based zeolite Y from Ahoko Nigeria using a novel metakaolinization technique. J. Dispers. Sci. Technol. 31, 442–448 (2010).
Yusof, A.M., Nizam, N.A., Rashid, N.A.A.: Hydrothermal conversion of rice husk ash to faujasite-types and NaA-type of zeolites. J. Porous Mater. 17, 39–47 (2010).
Tan, W.-C., Yap, S.-Y., Matsumoto, A., Othman, R., Yeoh, F.-Y.: Synthesis and characterization of zeolites NaA and NaY from rice husk ash. Adsorption. 17, 863–868 (2011).
Breck, D.W.: Crystalline zeolite Y, (1964)
Robson, H.: Verified synthesis of zeolitic materials. Elsevier Science (2001)
Image processing and analysis in Java: ImageJ. Software
H. van Bekkum, E.M. Flanigen, K.J.: Introduction to zeolite science and practice, Studies in Surface Science and Catalysis 137. Elsevier Science B.V, Delft (2001)
Byrappa, K., Yoshimura, M.: Handbook of Hydrothermal Technology. Elsevier, New York (2013)
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Received on 02/09/2019
Accepted on 15/10/2019
Published on 30/12/2019
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